di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Base Information

Chemical Name:di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate
CAS No.:1367824-37-0
Molecular Formula:C₂₂H₃₈NO₅PS
Molecular Weight:459.587
Hs Code.:

Synonyms:di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

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Chemical Property of di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Chemical Property:

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Technology Process of di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

There total 5 articles about di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1367824-36-9
diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

: 865-47-4
potassium tert-butylate

: 1367824-37-0
di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: In 1,4-dioxane; tert-butyl alcohol; at 20 ℃;

Reference yield:

: 27098-65-3
3-phenylsulfanyl-propionaldehyde

: 1367824-37-0
di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 1 h / 80 °C

2: hydrogen bromide; acetic acid / water

3: triethylamine / dichloromethane / 0 - 20 °C

4: 1,4-dioxane; tert-butyl alcohol / 20 °C

With hydrogen bromide; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 108-98-5
thiophenol

: 1367824-37-0
di-tert-butyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: acetic acid / 1 h / 80 °C

3: hydrogen bromide; acetic acid / water

4: triethylamine / dichloromethane / 0 - 20 °C

5: 1,4-dioxane; tert-butyl alcohol / 20 °C

With hydrogen bromide; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane; water; tert-butyl alcohol;