diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Base Information

Chemical Name:diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate
CAS No.:1367824-36-9
Molecular Formula:C₂₆H₃₀NO₅PS
Molecular Weight:499.568
Hs Code.:

Synonyms:diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

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Chemical Property of diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

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Technology Process of diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

There total 5 articles about diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1367824-34-7
[3-(phenylsulfanyl)-1-(RS)-(diphenoxyphosphoryl)propan-1-aminium] bromide

: 1367824-36-9
diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 52.0%

: 101-02-0
triphenyl phosphite

: 4248-19-5
tert-butyl carbazate

: 27098-65-3
3-phenylsulfanyl-propionaldehyde

: 1367824-36-9
diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 20 ℃;

Reference yield:

: 108-98-5
thiophenol

: 1367824-36-9
diphenyl [(RS)-1-(tert-butoxycarbonylamino)-3-(phenylsulfanyl)propyl]phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: acetic acid / 1 h / 80 °C

3: hydrogen bromide; acetic acid / water

4: triethylamine / dichloromethane / 0 - 20 °C

With hydrogen bromide; acetic acid; triethylamine; In dichloromethane; water;