4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

Base Information

Chemical Name:4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal
CAS No.:1262838-20-9
Molecular Formula:C₂₃H₃₈O₄
Molecular Weight:378.552
Hs Code.:

Synonyms:4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

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Chemical Property of 4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

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Technology Process of 4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

There total 6 articles about 4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1262838-30-1
4-(3,5-bis(hexyloxy)benzyloxy)-1-butanol

: 1262838-20-9
4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1246/cl.2010.1166

Reference yield:

: 111-25-1
1-bromo-hexane

: 1262838-20-9
4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 13 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: silver(l) oxide / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0.83 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; carbon tetrabromide; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1246/cl.2010.1166

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1262838-20-9
4-(3,5-bis(hexyloxy)benzyloxy)-1-butanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 13 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: silver(l) oxide / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0.83 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; carbon tetrabromide; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1246/cl.2010.1166