5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

Base Information

Chemical Name:5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine
CAS No.:1262838-21-0
Molecular Formula:C₂₇H₄₅N₅O₃
Molecular Weight:487.686
Hs Code.:

Synonyms:

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Chemical Property of 5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

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Technology Process of 5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

There total 9 articles about 5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1262838-32-3
2-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)propanedinitrile

: 50-01-1
guanidine hydrochloride

: 1262838-21-0
5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

Guidance literature:: guanidine hydrochloride; With ethanol; sodium; Inert atmosphere;

2-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)propanedinitrile; In ethanol; for 12h; Reflux; Inert atmosphere;
DOI:10.1246/cl.2010.1166

Reference yield:

: 1262838-30-1
4-(3,5-bis(hexyloxy)benzyloxy)-1-butanol

: 1262838-21-0
5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0.83 h / 0 - 20 °C / Inert atmosphere

2.1: aluminum oxide / toluene / 1 h / 20 °C

3.1: sodium tetrahydroborate / isopropyl alcohol / 1 h / 0 °C

4.1: ethanol; sodium / Inert atmosphere

4.2: 12 h / Reflux; Inert atmosphere

With aluminum oxide; sodium tetrahydroborate; ethanol; sodium; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; isopropyl alcohol; toluene;
DOI:10.1246/cl.2010.1166

Reference yield:

: 111-25-1
1-bromo-hexane

: 1262838-21-0
5-(4-(3,5-bis(hexyloxy)benzyloxy)butyl)-2,4,6-pyrimidinetriamine

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetonitrile / 13 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: silver(l) oxide / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0.83 h / 0 - 20 °C / Inert atmosphere

6.1: aluminum oxide / toluene / 1 h / 20 °C

7.1: sodium tetrahydroborate / isopropyl alcohol / 1 h / 0 °C

8.1: ethanol; sodium / Inert atmosphere

8.2: 12 h / Reflux; Inert atmosphere

With aluminum oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; ethanol; carbon tetrabromide; sodium; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene; acetonitrile;
DOI:10.1246/cl.2010.1166