1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

Base Information

Chemical Name:1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine
CAS No.:111515-85-6
Molecular Formula:C₂₃H₃₄N₂O₆Si
Molecular Weight:462.618
Hs Code.:

Synonyms:1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

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Technology Process of 1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

There total 21 articles about 1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124287-88-3
1-N-benzyl-1-N-(benzyloxycarbonyl)-6-O-(tert-butyldimethylsilyl)-4,5-N,O-carbonyl-3-de-O-methylfortamine

: 74-88-4
methyl iodide

: 111515-85-6
1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

Guidance literature:: With sodium hydride;
DOI:10.1246/cl.1987.29

Reference yield:

: 111515-80-1
methyl (1R,2R,4S,5R,6R)-4-azido-5-hydroxy-9-methyl-8-oxo-9-aza-7-oxabicyclo<4.3.0>nonanecarboxylate

: 111515-85-6
1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

Guidance literature:: Multi-step reaction with 8 steps

1: H₂ / Pd/C

2: NaHCO₃

3: 92 percent / imidazole

4: NaOH

5: 1.) 1-oxa-2-oxo-3-thia-indolizinium chloride, DMAP, CBrCl₃, 2.) DBU

6: NaH

7: OsO₄, trimethylamine N-oxide

8: 95 percent / NaH

With 1H-imidazole; dmap; sodium hydroxide; osmium(VIII) oxide; Bromotrichloromethane; trimethylamine-N-oxide; 1-oxa-2-oxo-3-thiaindolizinium chloride; hydrogen; sodium hydride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal;
DOI:10.1246/cl.1987.29

Reference yield:

: 124287-84-9
(1R,6S)-6-<(methoxycarbonyl)amino>cyclohex-3-enecarboxylic acid

: 111515-85-6
1-N-benzyl-6-O-(tert-butyldimethylsilyl)-1,2:4,5-di-N,O-carbonylfortamine

Guidance literature:: Multi-step reaction with 15 steps

1: 1.) I₂, KI, NaHCO₃, 2.) DBU

2: 95 percent / Ag₂O

4: triethylamine

5: 95 percent / 1,2-dichloro-ethane / Heating

6: 92 percent / MCPBA

7: TMSN₃, ZnCl₂

8: H₂ / Pd/C

9: NaHCO₃

10: 92 percent / imidazole

11: NaOH

12: 1.) 1-oxa-2-oxo-3-thia-indolizinium chloride, DMAP, CBrCl₃, 2.) DBU

13: NaH

14: OsO₄, trimethylamine N-oxide

15: 95 percent / NaH

With 1H-imidazole; dmap; sodium hydroxide; osmium(VIII) oxide; Bromotrichloromethane; trimethylamine-N-oxide; trimethylsilylazide; 1-oxa-2-oxo-3-thiaindolizinium chloride; hydrogen; iodine; sodium hydride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium iodide; zinc(II) chloride; silver(l) oxide; palladium on activated charcoal; In 1,2-dichloro-ethane;
DOI:10.1246/cl.1987.29