methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

Base Information

Chemical Name:methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate
CAS No.:1350766-31-2
Molecular Formula:C₁₃H₁₀ClNO₃S₂
Molecular Weight:327.812
Hs Code.:

Synonyms:methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

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Chemical Property of methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

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Technology Process of methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

There total 3 articles about methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-15-0,12122-00-8
carbon disulfide

: 104-86-9
4-chlorobenzylamine

: 762-42-5
dimethyl acetylenedicarboxylate

: 1350766-31-2
methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

Guidance literature:: carbon disulfide; 4-chlorobenzylamine; With hexafluoroisopropanol dispersed into the nanoporous SBA-15; at 20 ℃; for 0.00833333h;

dimethyl acetylenedicarboxylate; at 20 ℃; chemoselective reaction;
DOI:10.1016/j.jfluchem.2013.05.025

Reference yield:

: 52626-37-6
(4-chloro-benzyl)-dithiocarbamic acid

: 762-42-5
dimethyl acetylenedicarboxylate

: 1350766-31-2
methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

Guidance literature:: With β‐cyclodextrin; In water; at 20 ℃; for 0.283333h; Green chemistry;
DOI:10.1080/10610278.2014.890200

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 1350766-31-2
methyl 2-[3-((4-chlorophenyl)methyl)-4-oxo-2-thioxo-1,3-thiazolan-5-ylidene]ethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: β‐cyclodextrin / water / 0.01 h / 20 °C / Green chemistry

2: β‐cyclodextrin / water / 0.28 h / 20 °C / Green chemistry

With β‐cyclodextrin; In water;
DOI:10.1080/10610278.2014.890200