13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

Base Information

Chemical Name:13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene
CAS No.:128184-05-4
Molecular Formula:C₃₂H₃₅BrN₄O₆S₃
Molecular Weight:747.755
Hs Code.:

Synonyms:13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

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Chemical Property of 13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

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Technology Process of 13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

There total 2 articles about 13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 56187-04-3
1,4,7-tritosyl-1,4,7-triazaheptane

: 106967-42-4
4-bromo-2,6-bis(bromomethyl)pyridine

: 128184-05-4
13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

Guidance literature:: With potassium carbonate; In acetonitrile; for 18h; Inert atmosphere; Reflux;
DOI:10.1002/chem.202101701

Reference yield: 81.0%

: 106967-42-4
4-bromo-2,6-bis(bromomethyl)pyridine

: 52601-80-6
N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt

: 128184-05-4
13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

Guidance literature:: In N,N-dimethyl-formamide; at 75 ℃;

Reference yield: 56.2%

: 128184-05-4
13-bromo-3,6,9-tritosyl-3,6,9,15-tetraazabicyclo<9.3.1>pentadeca-1(15),11,13-triene

: 3,3’,6,6’,9,9’-hexatosyl-13,13’-bis(3,6,9,15-tetraazabicyclo[9.3.1]pentadeca)-1(15),1’(15’),11,11’,13,13’-hexene

Guidance literature:: With nickel(II) chloride hexahydrate; triphenylphosphine; zinc; In N,N-dimethyl-formamide; at 50 ℃; Inert atmosphere;
DOI:10.1002/chem.202101701