C₂₅H₂₄F₄O₄

Base Information

• Chemical Name: C₂₅H₂₄F₄O₄
• CAS No.: 1333327-29-9
• Molecular Formula: C₂₅H₂₄F₄O₄
• Molecular Weight: 464.457
• Mol file: 1333327-29-9.mol

Synonyms:C₂₅H₂₄F₄O₄

Chemical Property of C₂₅H₂₄F₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₄F₄O₄

There total 5 articles about C₂₅H₂₄F₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C21H16F4O4 (1333327-28-8) + ethyl iodide (75-03-6) → C25H24F4O4 (1333327-29-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.jfluchem.2011.07.021

Reference yield:

4-vinyl-benzaldehyde (1791-26-0) → C25H24F4O4 (1333327-29-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.1: oxalyl dichloride / dichloromethane / 20 °C

2.2: 0 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; oxalyl dichloride; caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.jfluchem.2011.07.021

Reference yield:

C9H4F4O (1333327-25-5) → C25H24F4O4 (1333327-29-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 20 °C / Cooling with ice

2.1: oxalyl dichloride / dichloromethane / 20 °C

2.2: 0 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

With sodium tetrahydroborate; oxalyl dichloride; caesium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.jfluchem.2011.07.021

upstream raw materials:

C₂₁H₁₆F₄O₄

ethyl iodide

C₁₁H₈F₄O₂

C₉H₄F₄O

Refernces