Technology Process of C44H39N3O4
There total 5 articles about C44H39N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; methanol;
at 20 ℃;
under 2068.65 Torr;
Inert atmosphere;
DOI:10.1021/jo301945f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetic acid; zinc; sodium acetate / 0.5 h / 70 - 120 °C
2: sodium phenyl-methanolate / 1.58 h / 20 - 230 °C
3: acetic acid; lead(IV) tetraacetate / 16 h / 20 °C
4: toluene-4-sulfonic acid / isopropyl alcohol / 16 h / Reflux
5: triethylamine; palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 20 °C / 2068.65 Torr / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; sodium acetate; lead(IV) tetraacetate; toluene-4-sulfonic acid; acetic acid; triethylamine; sodium phenyl-methanolate; zinc;
In
tetrahydrofuran; methanol; isopropyl alcohol;
1: |Knorr Pyrrole Synthesis;
DOI:10.1021/jo301945f
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium nitrite; acetic acid / water / 15 - 20 °C
2: acetic acid; zinc; sodium acetate / 0.5 h / 70 - 120 °C
3: sodium phenyl-methanolate / 1.58 h / 20 - 230 °C
4: acetic acid; lead(IV) tetraacetate / 16 h / 20 °C
5: toluene-4-sulfonic acid / isopropyl alcohol / 16 h / Reflux
6: triethylamine; palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 20 °C / 2068.65 Torr / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; sodium acetate; lead(IV) tetraacetate; toluene-4-sulfonic acid; acetic acid; triethylamine; sodium phenyl-methanolate; zinc; sodium nitrite;
In
tetrahydrofuran; methanol; water; isopropyl alcohol;
2: |Knorr Pyrrole Synthesis;
DOI:10.1021/jo301945f