1-(p-tolyl)-1-hexyne

Base Information

Chemical Name:1-(p-tolyl)-1-hexyne
CAS No.:180071-98-1
Molecular Formula:C₁₃H₁₆
Molecular Weight:172.27
Hs Code.:

Synonyms:1-(p-tolyl)-1-hexyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(p-tolyl)-1-hexyne

Chemical Property:

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Technology Process of 1-(p-tolyl)-1-hexyne

There total 25 articles about 1-(p-tolyl)-1-hexyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 624-31-7
4-tolyl iodide

: 693-02-7
hex-1-yne

: 180071-98-1
1-(p-tolyl)-1-hexyne

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; Schlenk technique; Glovebox;
DOI:10.1021/acs.organomet.8b00467

Reference yield: 94.0%

: 106-38-7
para-bromotoluene

: 693-02-7
hex-1-yne

: 180071-98-1
1-(p-tolyl)-1-hexyne

Guidance literature:: With potassium carbonate; di(3,4-methylenedioxyphenyl)(diisopropylamino)phosphine; palladium diacetate; In tetrahydrofuran; at 65 ℃; for 8h;
DOI:10.1021/jo049379o

Reference yield: 93.0%

: 32359-01-6
hexenylmagnesium bromide

: 106-38-7
para-bromotoluene

: 180071-98-1
1-(p-tolyl)-1-hexyne

Guidance literature:: With [Cu(N,N'-bis(diisopropylphosphino)-N,N'-dimethyl-2,6-diaminopyridine)Br]; isopropylmagnesium bromide; In tetrahydrofuran; at 50 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.7b00857