C₅₈H₇₀N₂O₂₄S

Base Information

Chemical Name:C₅₈H₇₀N₂O₂₄S
CAS No.:872120-80-4
Molecular Formula:C₅₈H₇₀N₂O₂₄S
Molecular Weight:1211.26
Hs Code.:

C<sub>58</sub>H<sub>70</sub>N<sub>2</sub>O<sub>24</sub>S

Synonyms:C₅₈H₇₀N₂O₂₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₇₀N₂O₂₄S

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Technology Process of C₅₈H₇₀N₂O₂₄S

There total 13 articles about C₅₈H₇₀N₂O₂₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 872120-79-1
C₅₃H₆₄N₂O₂₂S

: 123-76-2
levulinic acid

: 872120-80-4
C₅₈H₇₀N₂O₂₄S

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/anie.200501608

Reference yield:

: 872120-64-4
(1S,3R,4R,8S)-8-Hydroxy-3-[(S)-hydroxy-((R)-2-phenyl-[1,3]dioxolan-4-yl)-methyl]-1-phenylsulfanyl-2-oxa-5-aza-bicyclo[2.2.2]octan-6-one

: 872120-80-4
C₅₈H₇₀N₂O₂₄S

Guidance literature:: Multi-step reaction with 9 steps

1: pyridine; 4-dimethylaminopyridine / 3 h / 20 °C

2: 1.38 g / hydrazinium acetate / tetrahydrofuran / 1.33 h / 20 °C

3: 74 percent / BH₃*NMe₃; AlCl₃; molecular sieves 4 Angstroem / tetrahydrofuran / 6 h / 0 - 20 °C

4: 49 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; molecular sieves 3 Angstroem / various solvent(s) / 5 h / -80 °C

5: 79 percent / pyridine; 4-dimethylaminopyridine / 42 h / 40 °C

6: trimethylamine / acetonitrile; H₂O / 48 h / 40 °C

7: 380 mg / potassium carbonate / dimethylformamide / 3 h / 20 °C

8: 94 percent / zinc / tetrahydrofuran / 28 h / 20 °C

9: 95 percent / 1,3-dicyclohexylcabodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; aluminium trichloride; trifluorormethanesulfonic acid; trimethylamine-borane; 3 A molecular sieve; 4 A molecular sieve; hydrazinium monoacetate; potassium carbonate; dicyclohexyl-carbodiimide; zinc; trimethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.200501608

Reference yield:

: Acetic acid (1S,3R,4R,8S)-3-[(S)-acetoxy-((R)-2-phenyl-[1,3]dioxolan-4-yl)-methyl]-5-acetyl-6-oxo-1-phenylsulfanyl-2-oxa-5-aza-bicyclo[2.2.2]oct-8-yl ester

: 872120-80-4
C₅₈H₇₀N₂O₂₄S

Guidance literature:: Multi-step reaction with 8 steps

1: 1.38 g / hydrazinium acetate / tetrahydrofuran / 1.33 h / 20 °C

2: 74 percent / BH₃*NMe₃; AlCl₃; molecular sieves 4 Angstroem / tetrahydrofuran / 6 h / 0 - 20 °C

3: 49 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; molecular sieves 3 Angstroem / various solvent(s) / 5 h / -80 °C

4: 79 percent / pyridine; 4-dimethylaminopyridine / 42 h / 40 °C

5: trimethylamine / acetonitrile; H₂O / 48 h / 40 °C

6: 380 mg / potassium carbonate / dimethylformamide / 3 h / 20 °C

7: 94 percent / zinc / tetrahydrofuran / 28 h / 20 °C

8: 95 percent / 1,3-dicyclohexylcabodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; aluminium trichloride; trifluorormethanesulfonic acid; trimethylamine-borane; 3 A molecular sieve; 4 A molecular sieve; hydrazinium monoacetate; potassium carbonate; dicyclohexyl-carbodiimide; zinc; trimethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.200501608