N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

Base Information

Chemical Name:N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide
CAS No.:261899-62-1
Molecular Formula:C₁₂H₁₇NO₃
Molecular Weight:223.272
Hs Code.:

Synonyms:N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

Suppliers and Price of N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

There total 1 articles about N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 40478-49-7
3-(3-methoxyphenyl)propanoyl chloride

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 261899-62-1
N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c2cc35037h

Reference yield:

: 66644-32-4
[(1E)-2-iodo-1-methyl-vinyl]-benzene

: 261899-62-1
N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

: (Z)-1-(3-methoxyphenyl)-5-phenyl-4-hexen-3-one

: 1393114-19-6
(E)-1-(3-methoxyphenyl)-5-phenyl-4-hexen-3-one

Guidance literature:: [(1E)-2-iodo-1-methyl-vinyl]-benzene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 0.5h; Inert atmosphere;

N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide; In diethyl ether; pentane; at 0 ℃; for 2.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.06.082

Reference yield:

: 261899-62-1
N-methoxy-N-methyl 3-(3-methoxyphenyl)propionamide

: 1372559-34-6
5-(3-methoxyphenethyl)dihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / -78 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 2.17 h / 0 - 23 °C / Inert atmosphere

2.2: 0 - 23 °C / Inert atmosphere

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18 h / 23 °C / Inert atmosphere; Molecular sieve

With tetrapropylammonium perruthennate; borane-THF; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300494q