Ph₂PCH₂NH(t-Bu)

Base Information

• Chemical Name: Ph₂PCH₂NH(t-Bu)
• CAS No.: 126140-10-1
• Molecular Formula: C₁₇H₂₂NP
• Molecular Weight: 271.342
• Mol file: 126140-10-1.mol

Synonyms:Ph₂PCH₂NH(t-Bu)

Chemical Property of Ph₂PCH₂NH(t-Bu)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ph₂PCH₂NH(t-Bu)

There total 4 articles about Ph₂PCH₂NH(t-Bu) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tert-butylamine (75-64-9) + diphenylphosphinomethanol (5958-44-1) → Ph2PCH2NH(t-Bu) (126140-10-1)

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.03.006

Reference yield: 70.0%

tert-butylamino(diphenylphosphanyl)acetic acid (843664-57-3) → Ph2PCH2NH(t-Bu) (126140-10-1)

Guidance literature:

In chloroform-d1; at 20 ℃; for 1h;

DOI:10.1039/b412860e

Reference yield:

diphenylphosphane (829-85-6) → Ph2PCH2NH(t-Bu) (126140-10-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / diethyl ether / 24 h / 20 °C

2: 70 percent / CDCl₃ / 1 h / 20 °C

In diethyl ether; chloroform-d1;

DOI:10.1039/b412860e

upstream raw materials:

tert-butylamino(diphenylphosphanyl)acetic acid

diphenylphosphane

tert-butylamine

diphenylphosphinomethanol

Downstream raw materials:

diphenyl(methyl)phosphine

PtCl₂((C₆H₅)2PCH₂NHC(CH₃)3)2

cis-{Mo(CO)4(Ph₂PCH₂NH(t-Bu))2}