7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

Chemical Name:7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside
CAS No.:1229735-10-7
Molecular Formula:C₈₂H₉₇NO₂₃
Molecular Weight:1464.67
Hs Code.:

7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Synonyms:7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Chemical Property of 7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of 7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 1 articles about 7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1192261-13-4
7-octen-1-yl 2-O-benzyl-3-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-4,6-O-benzylidene-β-D-galactopyranoside

: 83025-11-0
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate

: 507-09-5
tiolacetic acid

: 1229735-10-7
7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: 7-octen-1-yl 2-O-benzyl-3-O-[4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-4,6-O-benzylidene-β-D-galactopyranoside; 3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; Molecular sieve;

tiolacetic acid; With pyridine; In diethyl ether; at 20 ℃; for 72h; stereoselective reaction;
DOI:10.1071/CH09058

Reference yield: 96.0%

: 1229735-10-7
7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

: 1263272-78-1
C₇₆H₉₁NO₂₀

Guidance literature:: 7-octen-1-yl 3-O-[3-O-(2-(N-acetyl)-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-4,6-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl]-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside; With methanol; sodium methylate; at 20 ℃; for 2h;

With Amberlite IR 120 (H⁺); In methanol; at 20 ℃;
DOI:10.1071/CH09058