1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole

Base Information

• Chemical Name: 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole
• CAS No.: 380152-24-9
• Molecular Formula: C₃₀H₃₀N₁₂O₂
• Molecular Weight: 590.647
• Mol file: 380152-24-9.mol

Synonyms:1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole

Chemical Property of 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole

Chemical Property:

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Technology Process of 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole

There total 1 articles about 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,4-bis(bromomethyl)benzene (623-24-5) + 2,2,2-tris(pyrazol-1-yl)ethanol (308847-52-1) → 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole (380152-24-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 24h; Heating;

DOI:10.1002/1099-0682(200203)2002:3<543::AID-EJIC543>3.0.CO;2-2

Reference yield: 84.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + silver tetrafluoroborate (14104-20-2) + 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole (380152-24-9) → (1,4-bis[tris(pyrazolyl)ethoxymethyl]benzene)Ag2(BF4)2(THF)

Guidance literature:

In tetrahydrofuran; (N2); a soln. of ligand added dropwise to a soln. of Ag salt, stirred; filtered, washed (THF), dried (vac.); elem. anal.;

DOI:10.1021/ic035207i

Reference yield: 79.0%

silver hexafluoroantimonate (26042-64-8) + 1-(2-(4-((2,2,2-tris(pyrazol-1-yl)ethoxy)methyl)benzyloxy)-1,1-di(pyrazol-1-yl)ethyl)pyrazole (380152-24-9) → (p-C6H4[CH2OCH2C(pyrazolyl)3]2(AgSbF6)2).infin.

Guidance literature:

In tetrahydrofuran; (N2); a soln. of ligand added dropwise to a soln. of Ag salt, stirred; filtered, washed (THF), dried (vac.); elem. anal.;

DOI:10.1021/ic035207i

upstream raw materials:

1,4-bis(bromomethyl)benzene

2,2,2-tris(pyrazol-1-yl)ethanol