(+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride

Base Information

Chemical Name:(+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride
CAS No.:154-98-3
Molecular Formula:C₉H₁₁Cl₂N*ClH
Molecular Weight:240.56
Hs Code.:
DSSTox Substance ID:DTXSID00968353

Synonyms:(+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride;2,4-Dichloroamphetamine HCl;154-98-3;Benzeneethanamine, 2,4-dichloro-alpha-methyl-, hydrochloride, (+-)-;53581-63-8;1-(2,4-Dichlorophenyl)-2-aminopropane hydrochloride;SCHEMBL2270392;DTXSID00968353;LS-30099;1-(2,4-dichlorophenyl)propan-2-amine;hydrochloride;1-(2,4-Dichlorophenyl)propan-2-amine--hydrogen chloride (1/1);Benzeneethanamine, 2,4-dichloro-alpha-methyl-, hydrochloride (1:1)

Suppliers and Price of (+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:239.003532
Heavy Atom Count:13
Complexity:141

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(CC1=C(C=C(C=C1)Cl)Cl)N.Cl

Technology Process of (+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride

There total 2 articles about (+-)-2,4-Dichloro-alpha-methylbenzeneethanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 52287-58-8
(E)-2,4-dichloro-1-(2-nitroprop-1-en-1-yl)benzene

: 154-98-3,53581-63-8
2-(2,4-dichloro-phenyl)-1-methyl-ethylamine; hydrochloride

Guidance literature:: (E)-2,4-dichloro-1-(2-nitroprop-1-en-1-yl)benzene; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1.16667h; Heating / reflux;

With water; In tetrahydrofuran;

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 154-98-3,53581-63-8
2-(2,4-dichloro-phenyl)-1-methyl-ethylamine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 3 h / 90 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C / Heating / reflux

With lithium aluminium tetrahydride; ammonium acetate; acetic acid; In tetrahydrofuran;