Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

Base Information

Chemical Name:Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat
CAS No.:73870-07-2
Molecular Formula:C₂₁H₂₃NO₇
Molecular Weight:401.416
Hs Code.:

Synonyms:Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

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Chemical Property of Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

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Technology Process of Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

There total 6 articles about Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58950-57-5
3-(2-ethoxycarbonylethyl)-4-formyl-5-methylpyrrole-2-carboxylate

: 73870-07-2
Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / pyridine; various solvent(s) / 5 h / 90 - 100 °C

2: 71 percent / 1) H₂ / 1) Raney - Ni / 1) MeOH, 2) 60 deg C, 30 min

3: 93 percent / HCl / 24 h / 25 °C

4: 82 percent / Na / 1) steam bath, 1 h, 2) 10 Torr, 3 h

5: 92 percent / HCl / 24 h / 25 °C

6: 1) SO₂Cl₂, 3) NaOAc/H₂O / 1) CH₂Cl₂, 0 deg C, 15 min, 2) 20 deg C, 75 min, 3) steam bath, 10 min, water

With hydrogenchloride; sulfuryl dichloride; water; hydrogen; sodium acetate; sodium; nickel; In pyridine;

Reference yield:

: 73870-02-7
Ethyl-3-(2-carboxyvinyl)-5-ethoxycarbonyl-2-methylpyrrol-4-propionat

: 73870-07-2
Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / 1) H₂ / 1) Raney - Ni / 1) MeOH, 2) 60 deg C, 30 min

2: 93 percent / HCl / 24 h / 25 °C

3: 82 percent / Na / 1) steam bath, 1 h, 2) 10 Torr, 3 h

4: 92 percent / HCl / 24 h / 25 °C

5: 1) SO₂Cl₂, 3) NaOAc/H₂O / 1) CH₂Cl₂, 0 deg C, 15 min, 2) 20 deg C, 75 min, 3) steam bath, 10 min, water

With hydrogenchloride; sulfuryl dichloride; water; hydrogen; sodium acetate; sodium; nickel;

Reference yield:

: 73870-06-1
Methyl-5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-2-methylpyrrol-3-propionat

: 73870-07-2
Methyl-5-benzyloxycarbonyl-2-formyl-4-(2-methoxycarbonylethyl)pyrrol-3-propionat

Guidance literature:: With sulfuryl dichloride; water; sodium acetate; Yield given. Multistep reaction; 1) CH₂Cl₂, 0 deg C, 15 min, 2) 20 deg C, 75 min, 3) steam bath, 10 min, water;