(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

Base Information

Chemical Name:(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine
CAS No.:1268685-03-5
Molecular Formula:C₂₂H₃₁NO₂
Molecular Weight:341.494
Hs Code.:

Synonyms:(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

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Chemical Property of (S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

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Technology Process of (S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

There total 4 articles about (S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1268685-02-4
(S)-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

: 106-95-6
allyl bromide

: 1268685-03-5
(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

Guidance literature:: With tetrabutylammomium bromide; sodium hydrogencarbonate; In acetonitrile; for 4h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.020

Reference yield:

: 1333213-22-1
C₁₆H₂₁NO₂

: 1268685-03-5
(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: cerium(III) chloride heptahydrate; zinc / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: tetrabutylammomium bromide; sodium hydrogencarbonate / acetonitrile / 4 h / Reflux; Inert atmosphere

With cerium(III) chloride heptahydrate; tetrabutylammomium bromide; sodium hydrogencarbonate; zinc; In tetrahydrofuran; acetonitrile; 1: Barbier reaction;
DOI:10.1016/j.tetlet.2010.12.020

Reference yield:

: 78008-36-3
(R)-2,3-cyclohexylideneglyceraldehyde

: 1268685-03-5
(S)-N-allyl-N-benzyl-1-((S)-1,4-dioxaspiro[4.5]decan-2-yl)but-3-en-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / diethyl ether / 0.5 h / 0 °C

2: cerium(III) chloride heptahydrate; zinc / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3: tetrabutylammomium bromide; sodium hydrogencarbonate / acetonitrile / 4 h / Reflux; Inert atmosphere

With cerium(III) chloride heptahydrate; tetrabutylammomium bromide; sodium hydrogencarbonate; magnesium sulfate; zinc; In tetrahydrofuran; diethyl ether; acetonitrile; 2: Barbier reaction;
DOI:10.1016/j.tetlet.2010.12.020