(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

Base Information

Chemical Name:(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide
CAS No.:1373438-73-3
Molecular Formula:C₁₈H₁₅Br₂N₃O₂
Molecular Weight:465.144
Hs Code.:

Synonyms:(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

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Technology Process of (E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

There total 4 articles about (E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1373439-06-5
1-(5-bromo-1H-indol-2-yl)propan-1-one

: 39635-10-4
2-hydroxy-5-bromobenzohydrazide

: 1373438-73-3
(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

Guidance literature:: With acetic acid; In propan-1-ol; Reflux;
DOI:10.1016/j.bmc.2012.10.002

Reference yield: 41.0%

: 1373438-73-3
(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

Guidance literature:

Reference yield:

: 7254-19-5
5-bromo-2-indolecarboxylic acid

: 1373438-73-3
(E)-5-bromo-N'-(1-(5-bromo-1H-indol-2-yl)propylidene)-2-hydroxybenzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: tetrahydrofuran / 16 h / 30 °C

3.1: acetic acid / propan-1-ol / Reflux

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; In tetrahydrofuran; propan-1-ol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.10.002