6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

Base Information

Chemical Name:6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide
CAS No.:219130-33-3
Molecular Formula:C₁₇H₁₇F₃N₄S
Molecular Weight:366.41
Hs Code.:

Synonyms:6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

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Chemical Property of 6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

Chemical Property:

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Technology Process of 6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

There total 3 articles about 6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219130-31-1
6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarboxamide

: 219130-33-3
6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

Guidance literature:: With Lawessons reagent; In toluene; Heating;
DOI:10.1016/S0960-894X(01)00805-8

Reference yield:

: 6271-78-9
6-chloro-3-pyridinecarboxamide

: 219130-33-3
6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Na₂CO₃ / dimethylformamide / 60 °C

2: Lawesson's reagent / toluene / Heating

With Lawessons reagent; sodium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0960-894X(01)00805-8

Reference yield:

: 15532-75-9
1-(3-Trifluoromethylphenyl)piperazine

: 219130-33-3
6-[4-[3-(trifluoromethyl)phenyl]-1-piperazinyl]-3-pyridinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Na₂CO₃ / dimethylformamide / 60 °C

2: Lawesson's reagent / toluene / Heating

With Lawessons reagent; sodium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0960-894X(01)00805-8