(S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester

Base Information

• Chemical Name: (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester
• CAS No.: 345910-97-6
• Molecular Formula: C₁₈H₂₀N₄O₆
• Molecular Weight: 388.38

Synonyms:(S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester

Chemical Property of (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester

Chemical Property:

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Technology Process of (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester

There total 1 articles about (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4,6-dimethoxy-1 ,3,5-triazine (3140-73-6) + N-Benzyloxycarbonyl-L-proline (1148-11-4) → (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester (345910-97-6)

Guidance literature:

With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ol015840c

Reference yield:

vinyl magnesium bromide (1826-67-1) + (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester (345910-97-6) → 2-acryloylpyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 3h;

DOI:10.1021/ol015840c

Reference yield:

ethylmagnesium bromide (925-90-6) + (S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-(4,6-dimethoxy-[1,3,5]triazin-2-yl) ester (345910-97-6) → N-benzyloxycarbonylpyrrolidin-2-yl-propan-1-one

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 3h;

DOI:10.1021/ol015840c

upstream raw materials:

2-chloro-4,6-dimethoxy-1 ,3,5-triazine

N-Benzyloxycarbonyl-L-proline

Downstream raw materials:

(S)-benzyl 2-(3-(4-methoxybenzyl)-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

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