{bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

Base Information

Chemical Name:{bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine
CAS No.:112817-48-8
Molecular Formula:C₁₆H₃₇BBr₂N₃P
Molecular Weight:473.083
Hs Code.:

Synonyms:{bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

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Chemical Property of {bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

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Technology Process of {bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

There total 1 articles about {bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 112794-90-8
{bromo(di-isopropylamino)boryl}-tert-butyl(dibromophosphino)amine

: 108-18-9
diisopropylamine

: 112817-48-8
{bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

: 7550-35-8
lithium bromide

Guidance literature:: With lithium butanide; In diethyl ether; hexane; addn. of soln. of i-Pr2NH in ether and soln. of Li-butanide in hexane at 20°C to B-compound at 0°C, stirred for 2 h at room temp.; filtration, removal of solvent, recrystn. from hexane at -70°C; elem. anal.;

Reference yield: 54.0%

: 112817-48-8
{bromo(di-isopropylamino)boryl}-{bromo(di-isopropylamino)phosphino}-tert-butylamine

: 7439-93-2
lithium

: 112795-10-5
1-tert-butyl-2,3-bis(di-isopropylamino)-1,2,3-azaphosphaboriridine

: 7550-35-8
lithium bromide

Guidance literature:: In tetrahydrofuran; stirred at 0°C for 3 h; evapn. to dryness, dissolved in hexane, filtration, distn. of filtrate (from ether at -70°C); elem. anal.;