(RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide

Base Information

• Chemical Name: (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide
• CAS No.: 1002358-22-6
• Molecular Formula: C₁₁H₁₇N₃O₂S
• Molecular Weight: 255.341
• Mol file: 1002358-22-6.mol

Synonyms:(RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide

Chemical Property of (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide

There total 4 articles about (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(RS)-S-(3-nitrophenyl)-N-(isopropylcarbamoyl)-S-methyl-sulfoximide (1002358-21-5) → (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide (1002358-22-6)

Guidance literature:

With hydrogenchloride; iron; In methanol; ethanol; water; at 60 ℃; for 2h;

Reference yield:

methyl 3-nitrophenyl sulfoxide (132016-29-6,146143-21-7,3272-42-2) → (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide (1002358-22-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium azide; sulfuric acid / dichloromethane / 24 h / 0 - 45 °C

1.2: 0 °C / pH 11

2.1: toluene / 111 h / 20 - 104 °C

3.1: hydrogenchloride; iron / methanol; ethanol; water / 2 h / 60 °C

With hydrogenchloride; sodium azide; sulfuric acid; iron; In methanol; ethanol; dichloromethane; water; toluene;

Reference yield:

imino(methyl)(3-nitrophenyl)-λ6-sulfanone (22133-02-4) → (RS)-S-(3-aminophenyl)-N-(isopropylcarbamoyl)-S-methylsulfoximide (1002358-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 111 h / 20 - 104 °C

2: hydrogenchloride; iron / methanol; ethanol; water / 2 h / 60 °C

With hydrogenchloride; iron; In methanol; ethanol; water; toluene;

upstream raw materials:

(RS)-S-(3-nitrophenyl)-N-(isopropylcarbamoyl)-S-methyl-sulfoximide

1-(methylsulfanyl)-3-nitrobenzene

methyl 3-nitrophenyl sulfoxide

imino(methyl)(3-nitrophenyl)-λ⁶-sulfanone