2-phenoxyethylthienylselenide

Base Information

Chemical Name:2-phenoxyethylthienylselenide
CAS No.:600715-02-4
Molecular Formula:C₁₂H₁₂OSSe
Molecular Weight:283.253
Hs Code.:

Synonyms:2-phenoxyethylthienylselenide

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Chemical Property of 2-phenoxyethylthienylselenide

Chemical Property:

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Technology Process of 2-phenoxyethylthienylselenide

There total 1 articles about 2-phenoxyethylthienylselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 188290-36-0,8014-23-1,25233-34-5
thiophene

: 589-10-6
phenoxyethyl bromide

: 85152-87-0
di(2-thienyl) diselenide

: 600715-02-4
2-phenoxyethylthienylselenide

: 1,2-bis(2-phenoxyethyl)diselane

Guidance literature:: thiophene; With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 1h;

With selenium; In tetrahydrofuran; at 20 ℃; for 1h;

phenoxyethyl bromide; In tetrahydrofuran; for 0.5h;
DOI:10.1016/S0022-328X(03)00450-9

Reference yield:

: 14264-16-5,53996-95-5,62075-39-2,39716-73-9
bis(triphenylphosphine)nickel(II) chloride

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 75-09-2
dichloromethane

: 600715-02-4
2-phenoxyethylthienylselenide

: PdCl₂(P(C₆H₅)3)2*2CH₂Cl₂

: [Pd2Cl2(μ-Cl)(μ-SeTh)(PPh3)2]

Guidance literature:: In benzene; byproducts: NiCl2; ligand was dissolved in benzene, added to benzene soln. of Pd- and Ni-complexes; filtered, concd. by evapn. upon stirring overnight, filtered, recrystd. from CH2Cl2, sepd.;
DOI:10.1016/S0022-328X(03)00450-9