di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

Base Information

Chemical Name:di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate
CAS No.:863562-04-3
Molecular Formula:C₂₄H₃₂Cl₂F₄N₂O₅
Molecular Weight:575.428
Hs Code.:

Synonyms:di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

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Chemical Property of di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

Chemical Property:

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Technology Process of di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

There total 5 articles about di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-{4-[bis-(2-methanesulfonyloxy-ethyl)-amino]-2,3,5,6-tetrafluoro-benzoylamino}-pentanedioic acid di-tert-butyl ester

: 863562-04-3
di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide;
DOI:10.1021/jm0502182

Reference yield:

: 863562-01-0
di-tert-butyl pentafluorobenzoyl-L-glutamate

: 863562-04-3
di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / N,N-dimethyl-acetamide / 144 h / 85 °C

2: Et₃N; DMAP / CH₂Cl₂ / 20 °C

3: LiCl / dimethylformamide

With dmap; triethylamine; lithium chloride; In dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1021/jm0502182

Reference yield:

: 863562-03-2
di-tert-butyl {4-[bis(2-hydroxyethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

: 863562-04-3
di-tert-butyl {4-[bis(2-chloroethyl)amino]-2,3,5,6-tetrafluorobenzoyl}-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; DMAP / CH₂Cl₂ / 20 °C

2: LiCl / dimethylformamide

With dmap; triethylamine; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0502182