Technology Process of C20H21NO7
There total 12 articles about C20H21NO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
formic acid;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tert-pentoxide / tetrahydrofuran / 2 h / 20 - 40 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C / Cooling with ice
2.1: 1,4-dioxane / 6 h / 20 °C
3.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 2 h / -78 °C
4.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 100 °C
5.1: sulfuric acid / formic acid / 3 h / 20 °C
With
sulfuric acid; sodium tert-pentoxide; caesium carbonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; formic acid; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 100 °C
2: sulfuric acid / formic acid / 3 h / 20 °C
With
sulfuric acid; caesium carbonate;
In
formic acid; N,N-dimethyl-formamide;