N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

Base Information

Chemical Name:N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide
CAS No.:713108-78-2
Molecular Formula:C₂₂H₃₁N₅O₄
Molecular Weight:429.519
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

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Chemical Property of N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

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Technology Process of N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

There total 2 articles about N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4530-37-4
N-t-butyloxycarbonylglycyl-L-phenylalanine

: 713108-78-2
N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / tetrahydrofuran / 0.5 h / 20 °C

2: dimethylformamide / 0.5 h

With dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b400220b

Reference yield:

: 5036-48-6
3-(1H-imidazol-1-yl)propan-1-amine

: 101697-71-6
Boc-Gly-Phe-OSu

: 713108-78-2
N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

Guidance literature:: In N,N-dimethyl-formamide; for 0.5h;
DOI:10.1039/b400220b

Reference yield: 93.5%

: fac-[Re(pyridine-2-carboxylato-5-carboxylic acid)(CO)₃(H₂O)]

: 713108-78-2
N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)-phenylalaninamide

: [Re(N-(tert-butoxycarbonyl)glycyl-N-(3-(imidazol-1-yl)propyl)phenylalanine)(5-carboxypyridine-2-carboxylate)(CO)3]

Guidance literature:: In methanol; water; a soln. of complex in methanol was added to a soln. of amide in water, the mixt. was stirred at room temp. for 13 h; column chromy. on silica;
DOI:10.1039/b400220b