tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate
CAS No.:1312793-98-8
Molecular Formula:C₂₄H₃₅N₃O₆
Molecular Weight:461.558
Hs Code.:

Synonyms:tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

There total 4 articles about tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 144036-19-1
3-cyclopentyloxy-4-methoxy benzoic acid chloride

: 187834-88-4
tert-butyl 4-(hydrazinecarbonyl)piperidine-1-carboxylate

: 1312793-98-8
tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 - 30 ℃; for 5h;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 2971-79-1
isonipecotic acid methyl ester

: 1312793-98-8
tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water

2: hydrazine / methanol / Reflux

3: triethylamine / N,N-dimethyl-formamide / 5 h / 0 - 30 °C

With sodium hydrogencarbonate; triethylamine; hydrazine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 124443-68-1
1-tert-Butyl 4-methyl piperidine-1,4-dicarboxylate

: 1312793-98-8
tert-butyl 4-(2-(3-cyclopentyloxy-4-methoxybenzoyl)hydrazinecarbonyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / methanol / Reflux

2: triethylamine / N,N-dimethyl-formamide / 5 h / 0 - 30 °C

With triethylamine; hydrazine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031