methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

Base Information

Chemical Name:methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate
CAS No.:1373521-17-5
Molecular Formula:C₁₉H₂₂N₄O₃S
Molecular Weight:386.475
Hs Code.:

Synonyms:methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

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Chemical Property of methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

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Technology Process of methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

There total 3 articles about methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 39687-95-1
isocyanoacetic acid methyl ester

: 107-11-9,30551-89-4
1-amino-2-propene

: 31167-21-2
2-(benzylthio)pyrimidin-4-ol

: 1373521-17-5
methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

Guidance literature:: In methanol; at 60 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tet.2018.04.058

Reference yield:

: 100-44-7
benzyl chloride

: 1373521-17-5
methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / 3 h / Reflux

2: methanol / Inert atmosphere; Reflux

With potassium carbonate; In methanol; water; 2: Ugi-Smiles coupling reaction;
DOI:10.1055/s-0031-1290347

Reference yield:

: 100-39-0
benzyl bromide

: 1373521-17-5
methyl 2-(2-(allyl(2-(benzylthio)pyrimidin-4-yl)amino)acetamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / 3 h / Reflux; Inert atmosphere

2: methanol / 48 h / 60 °C / Inert atmosphere

With potassium carbonate; In methanol; water; 2: |Ugi Condensation;
DOI:10.1016/j.tet.2018.04.058