4-O-(p-methoxybenzyl)aurodox

Base Information

Chemical Name:4-O-(p-methoxybenzyl)aurodox
CAS No.:94958-27-7
Molecular Formula:C₅₂H₇₀N₂O₁₃
Molecular Weight:931.133
Hs Code.:

Synonyms:4-O-(p-methoxybenzyl)aurodox

Suppliers and Price of 4-O-(p-methoxybenzyl)aurodox

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-O-(p-methoxybenzyl)aurodox

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-O-(p-methoxybenzyl)aurodox

There total 9 articles about 4-O-(p-methoxybenzyl)aurodox which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94958-21-1
{(2E,4E)-(6S,7R)-7-[(3aR,4S,6R,6aS)-2,2-Dimethyl-6-((E)-3-oxo-propenyl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-6-methoxy-5-methyl-octa-2,4-dienyl}-carbamic acid 2,2,2-trichloro-ethyl ester

: 94958-27-7
4-O-(p-methoxybenzyl)aurodox

Guidance literature:: Multi-step reaction with 7 steps

1: NaN(SiMe₃)2 / toluene / 0.5 h / -78 - 0 °C

2: Me₃SiI / CH₂Cl₂ / 0.03 h / 0 °C

3: amberlyst-15 / dimethylformamide; H₂O / 25 °C

4: n-Bu₄NI / tetrahydrofuran / 25 °C

5: Zn / tetrahydrofuran / 25 °C / pH 7.2

6: CH₂Cl₂ / 25 °C

With amberlyst-15; trimethylsilyl iodide; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; zinc; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00292a039

Reference yield:

: [(E)-4-(4-Benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridin-3-yl)-3-methyl-4-oxo-but-2-enyl]-triphenyl-phosphonium; bromide

: 94958-27-7
4-O-(p-methoxybenzyl)aurodox

Guidance literature:: Multi-step reaction with 7 steps

1: NaN(SiMe₃)2 / toluene / 0.5 h / -78 - 0 °C

2: Me₃SiI / CH₂Cl₂ / 0.03 h / 0 °C

3: amberlyst-15 / dimethylformamide; H₂O / 25 °C

4: n-Bu₄NI / tetrahydrofuran / 25 °C

5: Zn / tetrahydrofuran / 25 °C / pH 7.2

6: CH₂Cl₂ / 25 °C

With amberlyst-15; trimethylsilyl iodide; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; zinc; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00292a039

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 94958-27-7
4-O-(p-methoxybenzyl)aurodox

Guidance literature:: Multi-step reaction with 4 steps

1: n-Bu₄NI / tetrahydrofuran / 25 °C

2: Zn / tetrahydrofuran / 25 °C / pH 7.2

3: CH₂Cl₂ / 25 °C

With tetra-(n-butyl)ammonium iodide; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00292a039