5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

Base Information

Chemical Name:5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate
CAS No.:1314042-55-1
Molecular Formula:C₂₅H₂₈FN₃O₄S
Molecular Weight:485.579
Hs Code.:

Synonyms:5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

There total 4 articles about 5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314042-54-0
N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

: 98-59-9
p-toluenesulfonyl chloride

: 1314042-55-1
5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

Guidance literature:: With potassium carbonate; In ethyl acetate; at 25 - 35 ℃; Reflux;

Reference yield:

: 42558-54-3
Methyl 4-methyl-3-oxopentanoate

: 1314042-55-1
5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethyl sulfoxide / Reflux

2.1: copper(l) chloride; sulfuric acid / methanol / Reflux

3.1: nitric acid; sodium nitrite / 5 - 35 °C

3.3: 3 h

4.1: potassium carbonate / ethyl acetate / 25 - 35 °C / Reflux

With sulfuric acid; nitric acid; potassium carbonate; copper(l) chloride; sodium nitrite; In methanol; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 135878-36-3
N,N-diethyl-4-methyl-3-oxopentanamide

: 1314042-55-1
5-(diethylcarbamoyl)-4-(4-fluorophenyl)-6-isopropyl-pyrimidin-2-yl-4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) chloride; sulfuric acid / methanol / Reflux

2.1: nitric acid; sodium nitrite / 5 - 35 °C

2.3: 3 h

3.1: potassium carbonate / ethyl acetate / 25 - 35 °C / Reflux

With sulfuric acid; nitric acid; potassium carbonate; copper(l) chloride; sodium nitrite; In methanol; ethyl acetate;