N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

Base Information

Chemical Name:N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide
CAS No.:1314042-54-0
Molecular Formula:C₁₈H₂₂FN₃O₂
Molecular Weight:331.39
Hs Code.:

Synonyms:N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

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Chemical Property of N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

Chemical Property:

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Technology Process of N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

There total 3 articles about N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314042-53-9
N,N-diethyl-4-(4-fluorophenyl)-6-isopropyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxamide

: 1314042-54-0
N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

Guidance literature:: N,N-diethyl-4-(4-fluorophenyl)-6-isopropyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxamide; With nitric acid; sodium nitrite; at 5 - 35 ℃;

With acetic acid; In water;

With sodium hydroxide; In water; for 3h;

Reference yield:

: 42558-54-3
Methyl 4-methyl-3-oxopentanoate

: 1314042-54-0
N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethyl sulfoxide / Reflux

2.1: copper(l) chloride; sulfuric acid / methanol / Reflux

3.1: nitric acid; sodium nitrite / 5 - 35 °C

3.3: 3 h

With sulfuric acid; nitric acid; copper(l) chloride; sodium nitrite; In methanol; dimethyl sulfoxide;

Reference yield:

: 135878-36-3
N,N-diethyl-4-methyl-3-oxopentanamide

: 1314042-54-0
N,N-diethyl-4-(4-fluorophenyl)-2-hydroxy-6-isopropyl pyrimidine-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) chloride; sulfuric acid / methanol / Reflux

2.1: nitric acid; sodium nitrite / 5 - 35 °C

2.3: 3 h

With sulfuric acid; nitric acid; copper(l) chloride; sodium nitrite; In methanol;