6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:1029806-15-2
Molecular Formula:C₂₅H₂₈N₂O₃
Molecular Weight:404.509
Hs Code.:

Synonyms:6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

There total 4 articles about 6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1029806-14-1
6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-1,2,3,4-tetrahydroisoquinoline hydrochloride

: 1029806-15-2
6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With sodium cyanoborohydride; zinc(II) chloride; In methanol; water; at 20 ℃;

Reference yield:

: 606978-01-2
1-(4-Bromo-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester

: 1029806-15-2
6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / palladium diacetate; triphenylphosphine / isopropyl alcohol

2: hydrogenchloride / diethyl ether

3: sodium cyanoborohydride; zinc(II) chloride / methanol; water / 20 °C

With hydrogenchloride; sodium cyanoborohydride; sodium carbonate; zinc(II) chloride; palladium diacetate; triphenylphosphine; In methanol; diethyl ether; water; isopropyl alcohol; 1: Suzuki Coupling;

Reference yield:

: 163105-90-6
2-methoxypyridin-3-yl-boronic acid

: 1029806-15-2
6,7-dimethoxy-1-[4-(2-methoxypyridin-3-yl)benzyl]-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / palladium diacetate; triphenylphosphine / isopropyl alcohol

2: hydrogenchloride / diethyl ether

3: sodium cyanoborohydride; zinc(II) chloride / methanol; water / 20 °C

With hydrogenchloride; sodium cyanoborohydride; sodium carbonate; zinc(II) chloride; palladium diacetate; triphenylphosphine; In methanol; diethyl ether; water; isopropyl alcohol; 1: Suzuki Coupling;