C₄₈H₅₄N₈O₁₁S

Base Information

Chemical Name:C₄₈H₅₄N₈O₁₁S
CAS No.:1380111-23-8
Molecular Formula:C₄₈H₅₄N₈O₁₁S
Molecular Weight:951.07
Hs Code.:

C<sub>48</sub>H<sub>54</sub>N<sub>8</sub>O<sub>11</sub>S

Synonyms:C₄₈H₅₄N₈O₁₁S

Suppliers and Price of C₄₈H₅₄N₈O₁₁S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₅₄N₈O₁₁S

Chemical Property:

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Technology Process of C₄₈H₅₄N₈O₁₁S

There total 21 articles about C₄₈H₅₄N₈O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.9%

: 1380111-22-7
C₂₇H₃₂N₄O₉S

: 1380110-42-8
1-(((2R,3S)-3-amino-4-oxoazetidin-2-yl)-methyl)-3-((1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridin-2-yl)methyl)urea trifluoroacetic acid salt

: 1380111-23-8
C₄₈H₅₄N₈O₁₁S

Guidance literature:: With triethylamine; In acetonitrile; at 40 ℃; Celite;

Reference yield:

: 100-39-0
benzyl bromide

: 1380111-23-8
C₄₈H₅₄N₈O₁₁S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium hydroxide / methanol; water / 0.17 h / Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 0 °C

5: potassium iodide / N,N-dimethyl-formamide / 20 °C

6: hydrazine hydrate / ethanol / 1 h / Reflux

7: ethyl acetate / 2 h / 50 °C

8: potassium phosphate / dichloromethane; water / 1 h / 22 °C

9: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C

10: trifluoroacetic acid / 3 h / 0 °C

11: triethylamine / acetonitrile / 40 h / 20 °C

With potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380111-23-8
C₄₈H₅₄N₈O₁₁S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium hydroxide / methanol; water / 0.17 h / Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 0 °C

5: potassium iodide / N,N-dimethyl-formamide / 20 °C

6: hydrazine hydrate / ethanol / 1 h / Reflux

7: ethyl acetate / 2 h / 50 °C

8: potassium phosphate / dichloromethane; water / 1 h / 22 °C

9: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C

10: trifluoroacetic acid / 3 h / 0 °C

11: triethylamine / acetonitrile / 40 h / 20 °C

With potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z