3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

Base Information

Chemical Name:3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone
CAS No.:1213776-86-3
Molecular Formula:C₃₄H₄₈O₈
Molecular Weight:584.75
Hs Code.:

3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

Synonyms:3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

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Chemical Property of 3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

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Technology Process of 3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

There total 5 articles about 3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 35458-21-0
phlorisobutyrophenone

: 126-81-8
dimedone

: 78-84-2
isobutyraldehyde

: 1213776-86-3
3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

Guidance literature:: With L-proline; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2017.10.011

Reference yield:

: 83814-58-8
5,5-dimethyl-2-(2-methyl)propylidenecyclohexane-1,3-dione

: 35458-21-0
phlorisobutyrophenone

: 1213776-86-3
3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.ejmech.2015.06.001

Reference yield:

: C₁₇H₂₉NO₂

: 1213776-86-3
3-hydroxy-5,5-dimethyl-2-(2-methyl-1-(2,4,6-trihydroxy-3-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)-5-isobutyrylphenyl)propyl)cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; hydrogenchloride / dichloromethane; water / 0.08 h

2: sodium hydride / tetrahydrofuran / 20 °C

With hydrogenchloride; sodium hydride; ammonium chloride; In tetrahydrofuran; dichloromethane; water; 2: |Michael Addition;
DOI:10.1016/j.ejmech.2015.06.001