Technology Process of C58H36N6O
There total 3 articles about C58H36N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-chloro-4,6-diphenyl-1,3,5-triazine; C40H40B2O5;
With
potassium carbonate;
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate;
In
1,4-dioxane; toluene;
at 120 ℃;
for 24h;
Inert atmosphere;
With
sodium cyanide;
In
1,4-dioxane; water; toluene;
at 100 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide monohydrate / dichloromethane / 4 h / 25 °C
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chlorobenzene / 2 h / Reflux; Inert atmosphere
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 - 25 °C
4.1: potassium carbonate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene; 1,4-dioxane / 24 h / 120 °C / Inert atmosphere
4.2: 1 h / 100 °C
With
n-butyllithium; lithium hydroxide monohydrate; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; chlorobenzene; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chlorobenzene / 2 h / Reflux; Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 - 25 °C
3.1: potassium carbonate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene; 1,4-dioxane / 24 h / 120 °C / Inert atmosphere
3.2: 1 h / 100 °C
With
n-butyllithium; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane; hexane; chlorobenzene; toluene;