4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole

Base Information

• Chemical Name: 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole
• CAS No.: 369631-84-5
• Molecular Formula: C₂₁H₁₈BrNO₂S
• Molecular Weight: 428.349

Synonyms:4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole

Chemical Property of 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole

Chemical Property:

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Technology Process of 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole

There total 1 articles about 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[2-(benzo[b]thiophene-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole (325982-57-8) + trioxane (188680-60-6) + sodium hydrogencarbonate (144-55-8) → 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole (369631-84-5)

Guidance literature:

With hydrogen bromide; In dichloromethane; acetone;

Reference yield:

4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole (369631-84-5) + ethyl 2-methoxyacetate (3938-96-3) → 2-Methoxy-3-{4-[2-(5-methyl-2-phenyl-oxazol-4-yl)-ethoxyl]-benzo[b]thiophen-7-yl}-propionic acid ethyl ester (475480-83-2)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; diisopropylamine; In tetrahydrofuran;

Reference yield:

thiazoline-2,4-dione (2295-31-0) + t-butyl methylether + 4-[2-(7-Bromomethyl-benzo[b]thiophen-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole (369631-84-5) → 5-{4-[2-(5-methyl-2-phenyloxazol-4-yl)-ethoxy]-benzo[b]thiophen-7-ylmethyl}-thiazolidine-2,4-dione (892128-35-7,892128-36-8,213411-83-7)

Guidance literature:

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; water;

upstream raw materials:

4-[2-(benzo[b]thiophene-4-yloxy)-ethyl]-5-methyl-2-phenyl-oxazole

trioxane

sodium hydrogencarbonate

Downstream raw materials:

2-Methoxy-3-{4-[2-(5-methyl-2-phenyl-oxazol-4-yl)-ethoxyl]-benzo[b]thiophen-7-yl}-propionic acid ethyl ester

5-{4-[2-(5-methyl-2-phenyloxazol-4-yl)-ethoxy]-benzo[b]thiophen-7-ylmethyl}-thiazolidine-2,4-dione

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