Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester
CAS No.:57651-45-3
Molecular Formula:C₁₆H₂₄O₅S
Molecular Weight:328.43
Hs Code.:

Synonyms:Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

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Technology Process of Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

There total 3 articles about Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21461-86-9
(5R)-γ-valerolactone γ-carboxylic acid

: 57651-45-3
Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran / 60 °C

2: TsOH / 25 °C

3: pyridine / 0 °C

With pyridine; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1021/ja00395a061

Reference yield:

: 57651-43-1
(R)-1,2-O-isopropylidene-2-methyl-1,2,5-pentanetriol

: 98-59-9
p-toluenesulfonyl chloride

: 57651-45-3
Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

Guidance literature:: With pyridine; at 0 ℃;
DOI:10.1021/ja00395a061

Reference yield:

: 21461-88-1
(R)-2-methyl-pentane-1,2,5-triol

: 57651-45-3
Toluene-4-sulfonic acid 3-((R)-2,2,4-trimethyl-[1,3]dioxolan-4-yl)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / 25 °C

2: pyridine / 0 °C

With pyridine; toluene-4-sulfonic acid;
DOI:10.1021/ja00395a061