1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

Base Information

Chemical Name:1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole
CAS No.:645414-80-8
Molecular Formula:C₄₈H₃₆N₆
Molecular Weight:696.854
Hs Code.:

1,1',1''-tribenzyl-6-phenyl-1<i>H</i>,1'<i>H</i>,1''<i>H</i>-[2,5';2',5'']terbenzoimidazole

Synonyms:1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

Chemical Property:

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Technology Process of 1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

There total 10 articles about 1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 645414-75-1
1-benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzimidazole

: 645414-79-5
1,1'-dibenzyl-2'-iodo-6-phenyl-1H,1'H-[2,5']bibenzoimidazolyl

: 645414-80-8
1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1016/j.tetlet.2003.10.007

Reference yield:

: 21304-38-1
4-iodobenzene-1,2-diamine

: 645414-80-8
1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / KSF clay / toluene / Heating

2: KOH / acetone / 0 - 20 °C

3: 91 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / toluene / 75 °C

4: 81 percent / LDA; ICH₂CH₂I / tetrahydrofuran / -78 - 20 °C

5: 75 percent / K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 50 °C

6: 83 percent / LDA; ICH₂CH₂I / tetrahydrofuran / -78 - 20 °C

7: 79 percent / K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 50 °C

With potassium hydroxide; potassium phosphate; 1,2-Diiodoethane; KSF clay; sodium carbonate; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tetlet.2003.10.007

Reference yield:

: 100-39-0
benzyl bromide

: 645414-80-8
1,1',1''-tribenzyl-6-phenyl-1H,1'H,1''H-[2,5';2',5'']terbenzoimidazole

Guidance literature:: Multi-step reaction with 6 steps

1: KOH / acetone / 0 - 20 °C

2: 91 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / toluene / 75 °C

3: 81 percent / LDA; ICH₂CH₂I / tetrahydrofuran / -78 - 20 °C

4: 75 percent / K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 50 °C

5: 83 percent / LDA; ICH₂CH₂I / tetrahydrofuran / -78 - 20 °C

6: 79 percent / K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 50 °C

With potassium hydroxide; potassium phosphate; 1,2-Diiodoethane; sodium carbonate; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tetlet.2003.10.007