C₂₃H₂₀FN₉O

Base Information

Chemical Name:C₂₃H₂₀FN₉O
CAS No.:1431872-12-6
Molecular Formula:C₂₃H₂₀FN₉O
Molecular Weight:457.47
Hs Code.:

C<sub>23</sub>H<sub>20</sub>FN<sub>9</sub>O

Synonyms:C₂₃H₂₀FN₉O

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Chemical Property of C₂₃H₂₀FN₉O

Chemical Property:

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Technology Process of C₂₃H₂₀FN₉O

There total 11 articles about C₂₃H₂₀FN₉O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1431873-84-5
C₂₄H₂₂FN₉O₄S

: 74-89-5
methylamine

: 1431872-12-6
C₂₃H₂₀FN₉O

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; for 87h;

Reference yield:

: 1431872-97-7
C₇H₄BrN₃O

: 1431872-12-6
C₂₃H₂₀FN₉O

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

3.1: propan-1-ol / 1 h / 100 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C / Inert atmosphere

4.2: 48 h / 20 °C

5.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 87 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium hydroxide monohydrate; water; sodium hydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In tetrahydrofuran; propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1431872-96-6
C₈H₈ClN₃O₂

: 1431872-12-6
C₂₃H₂₀FN₉O

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

4.1: propan-1-ol / 1 h / 100 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 5 °C / Inert atmosphere

5.2: 48 h / 20 °C

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 87 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium hydroxide monohydrate; water; hydrogen bromide; sodium hydride; sodium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In tetrahydrofuran; propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;