9-Cinnamylidene fluorene

Base Information

• Chemical Name: 9-Cinnamylidene fluorene
• CAS No.: 2871-26-3
• Molecular Formula: C22H16
• Molecular Weight: 280.369
• NSC Number: 12315
• Nikkaji Number: J586.431C
• Mol file: 2871-26-3.mol

Synonyms:Cinnamalfluorene;2871-26-3;9-Cinnamylidene fluorene;9-CINNAMYLIDENEFLUORENE;Cinnamalfluoren;9-(3-Phenyl-2-propen-1-ylidene)-9H-fluorene;9-[(E)-3-phenylprop-2-enylidene]fluorene;FDELSKWIDIUQDN-DHZHZOJOSA-N;NSC12315;Fluorene, 9-cinnamylidene-, (E)-;NSC-12315;AKOS024319111;9-[(2E)-3-Phenyl-2-propenylidene]-9H-fluorene #

Chemical Property of 9-Cinnamylidene fluorene

Chemical Property:

• Vapor Pressure: 1.39E-09mmHg at 25°C
• Melting Point: 155 °C
• Refractive Index: 1.75
• Boiling Point: 498.5 °C at 760 mmHg
• Flash Point: 249.7 °C
• PSA: 0.00000
• Density: 1.196 g/cm³
• LogP: 5.81210
• Storage Temp.: −20°C
• XLogP3: 5.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 280.125200510
• Heavy Atom Count: 22
• Complexity: 399

Purity/Quality:

99% ^*data from raw suppliers

9-CINNAMYLIDENEFLUORENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C=CC=C2C3=CC=CC=C3C4=CC=CC=C42
• Isomeric SMILES: C1=CC=C(C=C1)/C=C/C=C2C3=CC=CC=C3C4=CC=CC=C42

Technology Process of 9-Cinnamylidene fluorene

There total 9 articles about 9-Cinnamylidene fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Phenyl-3--propen-(1)-ol-(3) (102705-70-4) → 9-cinnamylidene-fluorene (2871-26-3)

Guidance literature:

With potassium hydroxide; In ethanol;

DOI:10.1021/ja01503a049

Reference yield:

(E)-3-phenylpropenal (14371-10-9) → 9-cinnamylidene-fluorene (2871-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 2NMe₃>OH / pyridine

2: KOH / ethanol

With potassium hydroxide; N-benzyl-trimethylammonium hydroxide; In pyridine; ethanol;

DOI:10.1021/ja01503a049

Reference yield:

9H-fluorene (86-73-7) → 9-cinnamylidene-fluorene (2871-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 2NMe₃>OH / pyridine

2: KOH / ethanol

With potassium hydroxide; N-benzyl-trimethylammonium hydroxide; In pyridine; ethanol;

DOI:10.1021/ja01503a049

upstream raw materials:

9H-fluorene

sodium ethanolate

benzaldehyde

diethyl ether

Downstream raw materials:

9-(3-phenylpropyl)-9H-fluorene

9-(3-phenyl-propenyl)-fluorene