(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

Base Information

Chemical Name:(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine
CAS No.:1623767-09-8
Molecular Formula:C₂₈H₃₈ClN₃O₃Si
Molecular Weight:528.167
Hs Code.:

(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

Synonyms:(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

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Chemical Property of (R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

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Technology Process of (R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

There total 1 articles about (R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1623767-09-8
(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 150 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1623767-09-8
(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

: 1623767-10-1
(R)-(4-(3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepin-1-yl)-6-methylpyridin-2-yl)methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1623767-09-8
(R)-1-(2-(((tert-butyldimethylsilyl)oxy)methyl)-6-methylpyridin-4-yl)-3-(4-chloro-3-methoxyphenyl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

: 1623763-95-0
(R)-3-(4-chloro-3-methoxyphenyl)-1-(2-(fluoromethyl)-6-methylpyridin-4-yl)-6-methyl-5,6,8,9-tetrahydroimidazo[1,5-d][1,4]oxazepine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 13 h / 20 °C

With tetrabutyl ammonium fluoride; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane;