6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Base Information

Chemical Name:6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine
CAS No.:956235-66-8
Molecular Formula:C₂₁H₃₆N₂O₂S
Molecular Weight:380.595
Hs Code.:

Synonyms:6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

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Chemical Property of 6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Chemical Property:

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Technology Process of 6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

There total 13 articles about 6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

: 956235-65-7
2-(6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexyl)-1H-isoindole-1,3(2H)-dione

: 956235-66-8
6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: With hydrazine; In ethanol; at 60 ℃; for 4h;

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 956235-66-8
6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / tetrabutylammomium bromide / water / 5 h / 20 °C

2: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr

4: triethylamine / dichloromethane / 20 °C

5: sodium hydrogencarbonate / N,N-dimethyl-formamide / 17 h / 70 °C

6: sodium periodate / methanol; water / 18 h / 20 °C

7: hydrazine / ethanol / 4 h / 60 °C

With sodium hydroxide; sodium periodate; hydrogen; sodium hydrogencarbonate; triethylamine; hydrazine; palladium 10% on activated carbon; tetrabutylammomium bromide; cetyltributylphosphonium bromide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 956235-14-6
methyl 3-(cyclopentylthio)benzoate

: 956235-66-8
6-{2-[[3-(cyclopentylsulfinyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hydroxide; water / tetrahydrofuran / 4 h / 20 °C

1.2: pH 3

2.1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 74.25 h / 0 - 20 °C

3.1: tetrahydrofuran / 2 h / -30 - 20 °C

4.1: borane-THF / tetrahydrofuran / 20 °C / Heating / reflux

5.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 17 h / 70 °C

6.1: sodium periodate / methanol; water / 18 h / 20 °C

7.1: hydrazine / ethanol / 4 h / 60 °C

With lithium hydroxide; sodium periodate; borane-THF; oxalyl dichloride; water; sodium hydrogencarbonate; hydrazine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; chloroform; water; N,N-dimethyl-formamide;