Technology Process of C41H54N2O7
There total 5 articles about C41H54N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
formic acid;
With
acetic anhydride;
at 20 ℃;
for 1h;
Inert atmosphere;
C40H54N2O6;
In
tetrahydrofuran; ethyl acetate;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ja201133d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl acetamide / 0.5 h / 0 °C / Inert atmosphere
1.2: 20 h / 20 - 120 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
2.2: 4 h / 60 °C / Inert atmosphere
3.1: palladium on carbon; hydrogen / tetrahydrofuran; ethanol / 10 h / 20 °C
4.1: acetic anhydride / 1 h / 20 °C / Inert atmosphere
4.2: 1 h / 0 - 20 °C / Inert atmosphere
With
palladium on carbon; hydrogen; acetic anhydride; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1021/ja201133d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
1.2: 4 h / 60 °C / Inert atmosphere
2.1: palladium on carbon; hydrogen / tetrahydrofuran; ethanol / 10 h / 20 °C
3.1: acetic anhydride / 1 h / 20 °C / Inert atmosphere
3.2: 1 h / 0 - 20 °C / Inert atmosphere
With
palladium on carbon; hydrogen; acetic anhydride; potassium carbonate;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja201133d
