2-(2,3-DIMETHYLPHENYL)ETHANOL

Base Information

• Chemical Name: 2-(2,3-DIMETHYLPHENYL)ETHANOL
• CAS No.: 40420-17-5
• Molecular Formula: C10H14 O
• Molecular Weight: 150.221
• Hs Code.: 2906299090
• Mol file: 40420-17-5.mol

Synonyms:Phenethylalcohol, 2,3-dimethyl- (3CI); 2,3-Dimethylphenethyl alcohol

Chemical Property of 2-(2,3-DIMETHYLPHENYL)ETHANOL

Chemical Property:

• PSA: 20.23000
• LogP: 1.83820
• Solubility.: Dichloromethane, Ethyl Acetate

Purity/Quality:

95% ^*data from raw suppliers

2-(2,3-Dimethylphenyl)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

Useful:

• Uses: 2-(2,3-Dimethylphenyl)ethanol is an intermediate in the synthesis of 1,2,6-Trimethyl-phenanthrene (T796610). 1,2,6-Trimethylphenanthrene is a persistent organic pollutant (POP).

Technology Process of 2-(2,3-DIMETHYLPHENYL)ETHANOL

There total 3 articles about 2-(2,3-DIMETHYLPHENYL)ETHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxirane (75-21-8,99932-75-9) + 2,3-dimethylphenylmagnesium bromide (134640-85-0) → 2,3-dimethyl-phenethyl alcohol (40420-17-5)

Guidance literature:

With diethyl ether;

DOI:10.1002/hlca.19330160145

Reference yield:

2,3-Dimethylaniline (87-59-2) → 2,3-dimethyl-phenethyl alcohol (40420-17-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) aq. HCl, NaNO₂, (ii) KI

2: (i) EtMgBr, (ii) /BRN= 102378/, (iii) H₂SO₄

Reference yield:

oxirane (75-21-8,99932-75-9) + 1-iodo-2,3-dimethylbenzene (31599-60-7) → 2,3-dimethyl-phenethyl alcohol (40420-17-5)

Guidance literature:

Multistep reaction; (i) EtMgBr, (ii) /BRN= 102378/, (iii) H₂SO₄;

upstream raw materials:

oxirane

2,3-dimethylphenylmagnesium bromide

1-iodo-2,3-dimethylbenzene

2,3-Dimethylaniline

Downstream raw materials:

1-(5-bromo-3,4-dihydroquinolin-1(2H)-yl)-2-(2,3-dimethylphenethoxy)ethanone

α-(2,3-Dimethylphenaethyl)-β-oxopimelinsaeureaethylester

8-(2,3-Dimethyl-1-phenyl)-6-methyl-5-oxo-octansaeuremethylester

2,3-dimethyl-phenethyl bromide