C₂₂H₃₀N₂O₅

Base Information

Chemical Name:C₂₂H₃₀N₂O₅
CAS No.:1354014-34-8
Molecular Formula:C₂₂H₃₀N₂O₅
Molecular Weight:402.491
Hs Code.:

C<sub>22</sub>H<sub>30</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₀N₂O₅

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Chemical Property of C₂₂H₃₀N₂O₅

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Technology Process of C₂₂H₃₀N₂O₅

There total 1 articles about C₂₂H₃₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: 1354014-33-7
C₂₇H₃₅N₃O₄

: 1354014-34-8
C₂₂H₃₀N₂O₅

Guidance literature:: With acetyl chloride; at 0 - 20 ℃; for 19h; Inert atmosphere;
DOI:10.1021/ol203302f

Reference yield:

: 1354014-34-8
C₂₂H₃₀N₂O₅

: C₂₇H₃₀N₂O₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

1.2: 0.25 h / 0 °C / Inert atmosphere

2.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran; isopropyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

With sodium tetrahydroborate; potassium tert-butylate; acetic acid; In tetrahydrofuran; isopropyl alcohol; 1.1: Dieckmann reaction;
DOI:10.1021/ol203302f

Reference yield:

: 1354014-34-8
C₂₂H₃₀N₂O₅

: 1354014-47-3
C₂₅H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

1.2: 0.25 h / 0 °C / Inert atmosphere

2.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran; isopropyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; water; acetic acid; In tetrahydrofuran; isopropyl alcohol; 1.1: Dieckmann reaction;
DOI:10.1021/ol203302f