methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Base Information

Chemical Name:methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate
CAS No.:499157-68-5
Molecular Formula:C₁₃H₁₅F₃O₇S
Molecular Weight:372.319
Hs Code.:

Synonyms:methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

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Chemical Property of methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

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Technology Process of methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

There total 5 articles about methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 499157-67-4
methyl 3-[2-hydroxy-4-(methoxymethoxy)phenyl]propanoate

: 1493-13-6
trifluorormethanesulfonic acid

: 499157-68-5
methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.166667h;

Reference yield:

: 499157-67-4
methyl 3-[2-hydroxy-4-(methoxymethoxy)phenyl]propanoate

: 358-23-6
trifluoromethylsulfonic anhydride

: 499157-68-5
methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.03.028

Reference yield:

: 93-35-6
7-hydroxy-2H-chromen-2-one

: 499157-68-5
methyl 3-(4-(methoxymethoxy)-2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-isopropylethylamine / DMF (N,N-dimethyl-formamide) / 4 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; methanol / 0.33 h / 20 °C

2.2: 0.67 h / 60 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 7 h / 20 °C

4.1: pyridine / dichloromethane / 0.17 h / 0 °C

With pyridine; hydrogen; sodium hydride; N-isopropylethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); dichloromethane;