1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

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Chemical Name:1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride
CAS No.:1260242-59-8
Molecular Formula:C₄₃H₄₄ClNO₆*ClH
Molecular Weight:742.739
Hs Code.:

Synonyms:1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

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Chemical Property of 1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

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Technology Process of 1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

There total 10 articles about 1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1352713-66-6
1-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)-3-nitropropan-2-one

: 1260242-59-8
1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

Guidance literature:: 1-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)-3-nitropropan-2-one; With tin(II) chloride dihdyrate; In ethyl acetate; for 5h; Inert atmosphere; Reflux;

With hydrogenchloride; In diethyl ether; at 0 ℃;

Reference yield:

: 1352713-65-5
Br^(1-)*C₄₉H₅₄ClN₄O₆⁽¹⁺⁾

: 1260242-59-8
1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

Guidance literature:: With hydrogenchloride; water; In ethanol; dichloromethane; at 0 - 20 ℃; for 3.5h;

Reference yield:

: 1225430-39-6
2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)acetonitrile

: 1260242-59-8
1-amino-3-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenyl)propan-2-one hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide; water / ethanol / Reflux

1.2: 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5.25 h / 0 - 20 °C / Inert atmosphere

3.1: dichloromethane; diethyl ether / 3 h / -30 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: hydrogen bromide / dichloromethane; diethyl ether; water / 0.5 h / 0 °C

5.1: dichloromethane / 3 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride; water / dichloromethane; ethanol / 3.5 h / 0 - 20 °C

With hydrogenchloride; oxalyl dichloride; water; hydrogen bromide; sodium hydroxide; N,N-dimethyl-formamide; In diethyl ether; ethanol; dichloromethane; water;