(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide
CAS No.:1429383-30-1
Molecular Formula:C₁₈H₃₀ClNO₂SSi
Molecular Weight:388.046
Hs Code.:

Synonyms:(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

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Chemical Property of (R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

Chemical Property:

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Technology Process of (R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

There total 4 articles about (R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 153294-02-1
(R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)acetaldehyde

: 1429383-30-1
(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: With copper(II) sulfate; In dichloromethane; at 20 ℃; for 68h;

Reference yield:

: 153294-00-9
(R)-3-chloromandelic acid methyl ester

: 1429383-30-1
(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 9 h / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / diethyl ether; toluene / 1 h / -78 °C / Inert atmosphere

3: copper(II) sulfate / dichloromethane / 68 h / 20 °C

With 1H-imidazole; diisobutylaluminium hydride; copper(II) sulfate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 153294-01-0
methyl (2R)-{[tert-butyl(dimethyl)silyl]oxy}(3-chlorophenyl)ethanoate

: 1429383-30-1
(R)-N-((R)-2-(tert-butyldimethylsilyloxy)-2-(3-chlorophenyl)ethylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / diethyl ether; toluene / 1 h / -78 °C / Inert atmosphere

2: copper(II) sulfate / dichloromethane / 68 h / 20 °C

With diisobutylaluminium hydride; copper(II) sulfate; In diethyl ether; dichloromethane; toluene;