Technology Process of 4-hydroxy-3-(4-methoxyphenyl)quinolin-2(1H)-one
There total 6 articles about 4-hydroxy-3-(4-methoxyphenyl)quinolin-2(1H)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dimethyl sulfoxide;
at 60 ℃;
for 24h;
under 750.075 Torr;
Schlenk technique;
DOI:10.1021/ol401571r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere
2: silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 24 h / 60 °C / 750.08 Torr / Schlenk technique
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol401571r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere
3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere
4: silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 24 h / 60 °C / 750.08 Torr / Schlenk technique
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol401571r
